Acetal and ketal deprotection using montmorillonite K10: The first synthesis of syn-4,8-dioxatricyclo[5.1.0.0(3,5)]-2,6-octanedione

E C L  Gautier; A E  Graham; A  McKillop; S P  Standen; R J K  Taylor

Acetal and ketal deprotection using montmorillonite K10: The first synthesis of syn-4,8-dioxatricyclo[5.1.0.0(3,5)]-2,6-octanedione

E C L Gautier, A E Graham, A McKillop, S P Standen, R J K Taylor

Chemistry

Research output: Contribution to journal › Article › peer-review

Abstract

Montmorillonite K10 in dichloromethane at room temperature conveniently and efficiently converts acetals and ketals into the corresponding carbonyl compounds. The title dione (diepoxy-1-4-cyclohexanedione) has been prepared for the first time using this procedure. (C) 1997 Elsevier Science Ltd.

Original language	English
Pages (from-to)	1881-1884
Number of pages	4
Journal	Tetrahedron Letters
Volume	38
Issue number	11
Publication status	Published - 17 Mar 1997

Keywords

SUPPORTED FERRIC NITRATE
CATALYST
CLEAVAGE

Cite this

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title = "Acetal and ketal deprotection using montmorillonite K10: The first synthesis of syn-4,8-dioxatricyclo[5.1.0.0(3,5)]-2,6-octanedione",

abstract = "Montmorillonite K10 in dichloromethane at room temperature conveniently and efficiently converts acetals and ketals into the corresponding carbonyl compounds. The title dione (diepoxy-1-4-cyclohexanedione) has been prepared for the first time using this procedure. (C) 1997 Elsevier Science Ltd.",

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year = "1997",

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pages = "1881--1884",

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T1 - Acetal and ketal deprotection using montmorillonite K10: The first synthesis of syn-4,8-dioxatricyclo[5.1.0.0(3,5)]-2,6-octanedione

AU - Gautier, E C L

AU - Graham, A E

AU - McKillop, A

AU - Standen, S P

AU - Taylor, R J K

PY - 1997/3/17

Y1 - 1997/3/17

N2 - Montmorillonite K10 in dichloromethane at room temperature conveniently and efficiently converts acetals and ketals into the corresponding carbonyl compounds. The title dione (diepoxy-1-4-cyclohexanedione) has been prepared for the first time using this procedure. (C) 1997 Elsevier Science Ltd.

AB - Montmorillonite K10 in dichloromethane at room temperature conveniently and efficiently converts acetals and ketals into the corresponding carbonyl compounds. The title dione (diepoxy-1-4-cyclohexanedione) has been prepared for the first time using this procedure. (C) 1997 Elsevier Science Ltd.

KW - SUPPORTED FERRIC NITRATE

KW - CATALYST

KW - CLEAVAGE

M3 - Article

SN - 0040-4039

VL - 38

SP - 1881

EP - 1884

JO - Tetrahedron Letters

JF - Tetrahedron Letters

IS - 11

ER -