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Acetic Anhydride/Et3N/DMAP: An Effective Acetylating System for Hemiacetals
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| Journal | SYNTHETIC COMMUNICATIONS |
|---|---|
| Date | Published - Jan 2011 |
| Issue number | 8 |
| Volume | 41 |
| Number of pages | 6 |
| Pages (from-to) | 1175-1180 |
| Original language | English |
Abstract
[image omitted] The selective and efficient acetylation of the hemiacetal hydroxyl in the equilibrium mixture between RCl2C(OAll)OH and AllOH/RCl2CHO was achieved using the acylating system Ac2O/Et3N/dimethylaminopyridine (DMAP).
- Acetylation, DMAP, haloaldehyde, hemiacetal, Ueno-Stork, TRANSFER RADICAL CYCLIZATION, COMPLEXES, CATALYST, ALCOHOLS, ROUTE, ATRC
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