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From the same journal

AN EFFICIENT, SIMPLE AND INEXPENSIVE METHOD FOR THE PREPARATION OF 1,4-BENZOQUINONE MONOKETALS VIA ANODIC-OXIDATION OF 1,4-DIMETHOXYBENZENES

Research output: Contribution to journalArticle

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Publication details

JournalSYNTHETIC COMMUNICATIONS
DatePublished - 1994
Issue number20
Volume24
Number of pages20
Pages (from-to)2989-3008
Original languageEnglish

Abstract

Anodic oxidation of a series of 1-substituted-2,5-dimethoxybenzenes gives 2-substituted-1,1,4,4-tetramethoxycyclohexa-2,5-dienes in almost quantitative crude yield. Selective monohydrolysis of these bis-ketals is possible in many cases, and gives 3-substituted-4,4-dimethoxycyclohexa-2,5-dienones in good to excellent overall yield.

    Research areas

  • QUINONE BISKETALS, ETHERS, ROUTE

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