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Definitive evidence for a pairwise addition of hydrogen to a platinum bis(phosphine) complex using parahydrogen-induced polarization

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Publication details

JournalOrganometallics
DatePublished - 25 Jun 1996
Issue number13
Volume15
Number of pages3
Pages (from-to)2863-2865
Original languageEnglish

Abstract

Through the use of parahydrogen-induced polarization (PHIP), conclusive evidence has been obtained that H-2 addition to Pt(Ph(2)PCH(2)CH(Me)OPPh(2)) proceeds in a concerted, pairwise manner. PHIP has also been used in. conjunction with a 2D HMQC sequence to obtain P-31 and Pt-195 NMR spectra from submilligram samples in 2-5 min.

    Research areas

  • OXIDATIVE-ADDITION, IRIDIUM(I) COMPLEXES, KINETIC CONTROL, CIS-DIHYDRIDE, SPIN, RESONANCE

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