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Loss of internal 1->6 substituted monosaccharide residues from underivatized and per-O-methylated trisaccharides

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Loss of internal 1->6 substituted monosaccharide residues from underivatized and per-O-methylated trisaccharides. / Brull, L P ; Heerma, W ; Thomas-Oates, Jane Elizabeth; Haverkamp, J ; Kovacik, V ; Kovac, P .

In: JOURNAL OF THE AMERICAN SOCIETY FOR MASS SPECTROMETRY, Vol. 8, No. 1, 01.1997, p. 43-49.

Research output: Contribution to journalArticle

Harvard

Brull, LP, Heerma, W, Thomas-Oates, JE, Haverkamp, J, Kovacik, V & Kovac, P 1997, 'Loss of internal 1->6 substituted monosaccharide residues from underivatized and per-O-methylated trisaccharides', JOURNAL OF THE AMERICAN SOCIETY FOR MASS SPECTROMETRY, vol. 8, no. 1, pp. 43-49.

APA

Brull, L. P., Heerma, W., Thomas-Oates, J. E., Haverkamp, J., Kovacik, V., & Kovac, P. (1997). Loss of internal 1->6 substituted monosaccharide residues from underivatized and per-O-methylated trisaccharides. JOURNAL OF THE AMERICAN SOCIETY FOR MASS SPECTROMETRY, 8(1), 43-49.

Vancouver

Brull LP, Heerma W, Thomas-Oates JE, Haverkamp J, Kovacik V, Kovac P. Loss of internal 1->6 substituted monosaccharide residues from underivatized and per-O-methylated trisaccharides. JOURNAL OF THE AMERICAN SOCIETY FOR MASS SPECTROMETRY. 1997 Jan;8(1):43-49.

Author

Brull, L P ; Heerma, W ; Thomas-Oates, Jane Elizabeth ; Haverkamp, J ; Kovacik, V ; Kovac, P . / Loss of internal 1->6 substituted monosaccharide residues from underivatized and per-O-methylated trisaccharides. In: JOURNAL OF THE AMERICAN SOCIETY FOR MASS SPECTROMETRY. 1997 ; Vol. 8, No. 1. pp. 43-49.

Bibtex - Download

@article{25377c4a0c5e4237ad31aa8c49944abd,
title = "Loss of internal 1->6 substituted monosaccharide residues from underivatized and per-O-methylated trisaccharides",
abstract = "The fragmentation behavior of [M + H](+) ions of a series of underivatized and per-O-methylated trisaccharides having 1 --> 6 linked residues, of which one or two is a deoxy-fluoro or deoxy residue and thus has a unique mass, has been studied by using collision-induced dissociation fast-atom bombardment mass spectrometry. In addition to the usual fragment ions resulting from glycosidic bond cleavage, fragment ions were observed which must have been generated following an unusual rearrangement process which can be rationalized in terms of the loss of an internal monosaccharide residue. (C) 1997 American Society for Mass Spectrometry",
keywords = "FAST-ATOM-BOMBARDMENT, TANDEM MASS-SPECTROMETRY, BETA-GLYCOSIDES, INDUCED DISSOCIATION, OLIGOSACCHARIDE CHARACTERIZATION, (1->6)-BETA-D-GALACTOOLIGOSACCHARIDES, FAB, O-(3-DEOXY-3-FLUORO-BETA-D-GALACTOPYRANOSYL)-(1->6)-O-BETA-D-GALACTOPYRANOSYL-(., (1->6)-BETA-D-GALACTO-OLIGOSACCHARIDES, SPECTRA",
author = "Brull, {L P} and W Heerma and Thomas-Oates, {Jane Elizabeth} and J Haverkamp and V Kovacik and P Kovac",
year = "1997",
month = "1",
language = "English",
volume = "8",
pages = "43--49",
journal = "JOURNAL OF THE AMERICAN SOCIETY FOR MASS SPECTROMETRY",
issn = "1044-0305",
publisher = "Springer New York",
number = "1",

}

RIS (suitable for import to EndNote) - Download

TY - JOUR

T1 - Loss of internal 1->6 substituted monosaccharide residues from underivatized and per-O-methylated trisaccharides

AU - Brull, L P

AU - Heerma, W

AU - Thomas-Oates, Jane Elizabeth

AU - Haverkamp, J

AU - Kovacik, V

AU - Kovac, P

PY - 1997/1

Y1 - 1997/1

N2 - The fragmentation behavior of [M + H](+) ions of a series of underivatized and per-O-methylated trisaccharides having 1 --> 6 linked residues, of which one or two is a deoxy-fluoro or deoxy residue and thus has a unique mass, has been studied by using collision-induced dissociation fast-atom bombardment mass spectrometry. In addition to the usual fragment ions resulting from glycosidic bond cleavage, fragment ions were observed which must have been generated following an unusual rearrangement process which can be rationalized in terms of the loss of an internal monosaccharide residue. (C) 1997 American Society for Mass Spectrometry

AB - The fragmentation behavior of [M + H](+) ions of a series of underivatized and per-O-methylated trisaccharides having 1 --> 6 linked residues, of which one or two is a deoxy-fluoro or deoxy residue and thus has a unique mass, has been studied by using collision-induced dissociation fast-atom bombardment mass spectrometry. In addition to the usual fragment ions resulting from glycosidic bond cleavage, fragment ions were observed which must have been generated following an unusual rearrangement process which can be rationalized in terms of the loss of an internal monosaccharide residue. (C) 1997 American Society for Mass Spectrometry

KW - FAST-ATOM-BOMBARDMENT

KW - TANDEM MASS-SPECTROMETRY

KW - BETA-GLYCOSIDES

KW - INDUCED DISSOCIATION

KW - OLIGOSACCHARIDE CHARACTERIZATION

KW - (1->6)-BETA-D-GALACTOOLIGOSACCHARIDES

KW - FAB

KW - O-(3-DEOXY-3-FLUORO-BETA-D-GALACTOPYRANOSYL)-(1->6)-O-BETA-D-GALACTOPYRANOSYL-(.

KW - (1->6)-BETA-D-GALACTO-OLIGOSACCHARIDES

KW - SPECTRA

M3 - Article

VL - 8

SP - 43

EP - 49

JO - JOURNAL OF THE AMERICAN SOCIETY FOR MASS SPECTROMETRY

T2 - JOURNAL OF THE AMERICAN SOCIETY FOR MASS SPECTROMETRY

JF - JOURNAL OF THE AMERICAN SOCIETY FOR MASS SPECTROMETRY

SN - 1044-0305

IS - 1

ER -