Simple preparation of novel metal-containing mesoporous starches

Manuel Ojeda; Vitaliy Budarin; Peter S. Shuttleworth; James H. Clark; Antonio Pineda; Alina M. Balu; Antonio A. Romero; Rafael Luque

doi:10.3390/ma6051891

Simple preparation of novel metal-containing mesoporous starches

Manuel Ojeda, Vitaliy Budarin, Peter S. Shuttleworth, James H. Clark, Antonio Pineda, Alina M. Balu, Antonio A. Romero, Rafael Luque^*

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

Abstract

Metal-containing mesoporous starches have been synthesized using a simple and efficient microwave-assisted methodology followed by metal impregnation in the porous gel network. Final materials exhibited surface areas >60 m² g^-1, being essentially mesoporous with pore sizes in the 10-15 nm range with some developed inter-particular mesoporosity. These materials characterized by several techniques including XRD, SEM, TG/DTA and DRIFTs may find promising catalytic applications due to the presence of (hydr)oxides in their composition.

Original language	English
Pages (from-to)	1891-1902
Number of pages	12
Journal	Materials
Volume	6
Issue number	5
DOIs	https://doi.org/10.3390/ma6051891
Publication status	Published - 10 May 2013

Keywords

Co
Cu
Fe
Mesoporous polysaccharides
Starch

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10.3390/ma6051891

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title = "Simple preparation of novel metal-containing mesoporous starches",

abstract = "Metal-containing mesoporous starches have been synthesized using a simple and efficient microwave-assisted methodology followed by metal impregnation in the porous gel network. Final materials exhibited surface areas >60 m2 g-1, being essentially mesoporous with pore sizes in the 10-15 nm range with some developed inter-particular mesoporosity. These materials characterized by several techniques including XRD, SEM, TG/DTA and DRIFTs may find promising catalytic applications due to the presence of (hydr)oxides in their composition.",

keywords = "Co, Cu, Fe, Mesoporous polysaccharides, Starch",

author = "Manuel Ojeda and Vitaliy Budarin and Shuttleworth, {Peter S.} and Clark, {James H.} and Antonio Pineda and Balu, {Alina M.} and Romero, {Antonio A.} and Rafael Luque",

year = "2013",

month = may,

day = "10",

doi = "10.3390/ma6051891",

language = "English",

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pages = "1891--1902",

journal = "Materials",

issn = "1996-1944",

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T1 - Simple preparation of novel metal-containing mesoporous starches

AU - Ojeda, Manuel

AU - Budarin, Vitaliy

AU - Shuttleworth, Peter S.

AU - Clark, James H.

AU - Pineda, Antonio

AU - Balu, Alina M.

AU - Romero, Antonio A.

AU - Luque, Rafael

PY - 2013/5/10

Y1 - 2013/5/10

N2 - Metal-containing mesoporous starches have been synthesized using a simple and efficient microwave-assisted methodology followed by metal impregnation in the porous gel network. Final materials exhibited surface areas >60 m2 g-1, being essentially mesoporous with pore sizes in the 10-15 nm range with some developed inter-particular mesoporosity. These materials characterized by several techniques including XRD, SEM, TG/DTA and DRIFTs may find promising catalytic applications due to the presence of (hydr)oxides in their composition.

AB - Metal-containing mesoporous starches have been synthesized using a simple and efficient microwave-assisted methodology followed by metal impregnation in the porous gel network. Final materials exhibited surface areas >60 m2 g-1, being essentially mesoporous with pore sizes in the 10-15 nm range with some developed inter-particular mesoporosity. These materials characterized by several techniques including XRD, SEM, TG/DTA and DRIFTs may find promising catalytic applications due to the presence of (hydr)oxides in their composition.

KW - Co

KW - Cu

KW - Fe

KW - Mesoporous polysaccharides

KW - Starch

UR - http://www.scopus.com/inward/record.url?scp=84881298393&partnerID=8YFLogxK

U2 - 10.3390/ma6051891

DO - 10.3390/ma6051891

M3 - Article

AN - SCOPUS:84881298393

SN - 1996-1944

VL - 6

SP - 1891

EP - 1902

JO - Materials

JF - Materials

IS - 5

ER -

Simple preparation of novel metal-containing mesoporous starches

Abstract

Keywords

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