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The Right Light – De Novo Design of a Robust Modular Photochemical Reactor for Optimum Batch and Flow Chemistry

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Author(s)

  • Gideon James Grogan
  • Holly Bonfield
  • Kayleigh Mercer
  • Alba Diaz-Rodriguez
  • Gemma Cook
  • Blandine McKay
  • Pawel Slade
  • George Taylor
  • Wei Xiang Ooi
  • Jason Williams
  • Jack Roberts
  • John Murphy
  • Luca Schmermund
  • Wolfgang Kroutil
  • Tamara Mielke
  • Jared Cartwright
  • Lee Edwards

Department/unit(s)

Publication details

JournalChemphotochem
DateAccepted/In press - 14 Aug 2019
DateE-pub ahead of print (current) - 15 Aug 2019
Early online date15/08/19
Original languageEnglish

Abstract

Having identified inconsistencies when repeating literature examples of photochemical transformations and difficulties recreating experimental setups, we devised several criteria that an ideal labscale reactor should achieve. Herein, we introduce a versatile photoreactor for high throughput screening, preparative scale batch reactions and continuous processing, all with a single light source. The reactor utilizes interchangeable arrays of pseudo-monochromatic high-power LEDs in a range of synthetically useful wavelengths, combined with excellent temperature control. Moreover, light intensity can be modulated in an accurate and straightforward manner. This system has subsequently been tested on a range of literature methodologies.

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