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Truncated dipolar recoupling in solid-state nuclear magnetic resonance

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Truncated dipolar recoupling in solid-state nuclear magnetic resonance. / Marin-Montesinos, Ildefonso; Mollica, Giulia; Carravetta, Marina; Gansmueller, Axel; Pilelo, Giuseppe; Bechmann, Matthias; Sebald, Angelika; Levitt, Malcolm H.

In: Chemical Physics Letters, Vol. 432, No. 4-6, 11.12.2006, p. 572-578.

Research output: Contribution to journalArticle

Harvard

Marin-Montesinos, I, Mollica, G, Carravetta, M, Gansmueller, A, Pilelo, G, Bechmann, M, Sebald, A & Levitt, MH 2006, 'Truncated dipolar recoupling in solid-state nuclear magnetic resonance', Chemical Physics Letters, vol. 432, no. 4-6, pp. 572-578. https://doi.org/10.1016/j.cplett.2006.10.101

APA

Marin-Montesinos, I., Mollica, G., Carravetta, M., Gansmueller, A., Pilelo, G., Bechmann, M., Sebald, A., & Levitt, M. H. (2006). Truncated dipolar recoupling in solid-state nuclear magnetic resonance. Chemical Physics Letters, 432(4-6), 572-578. https://doi.org/10.1016/j.cplett.2006.10.101

Vancouver

Marin-Montesinos I, Mollica G, Carravetta M, Gansmueller A, Pilelo G, Bechmann M et al. Truncated dipolar recoupling in solid-state nuclear magnetic resonance. Chemical Physics Letters. 2006 Dec 11;432(4-6):572-578. https://doi.org/10.1016/j.cplett.2006.10.101

Author

Marin-Montesinos, Ildefonso ; Mollica, Giulia ; Carravetta, Marina ; Gansmueller, Axel ; Pilelo, Giuseppe ; Bechmann, Matthias ; Sebald, Angelika ; Levitt, Malcolm H. / Truncated dipolar recoupling in solid-state nuclear magnetic resonance. In: Chemical Physics Letters. 2006 ; Vol. 432, No. 4-6. pp. 572-578.

Bibtex - Download

@article{e4dfeb1bc4ab4c3d84b1f09fb3246672,
title = "Truncated dipolar recoupling in solid-state nuclear magnetic resonance",
abstract = "We describe a solid-state NMR concept for the estimation of individual spin-spin couplings in strongly-coupled homonuclear spin systems. A radiofrequency pulse sequence, synchronised with the magic-angle sample rotation recouples zero-quantum dipolar interactions as well as a frequency-dispersing interaction such as the chemical shift anisotropy. The combination of these two recoupled interactions causes the spin system to behave in an approximately weakly-coupled fashion. Individual spin-spin couplings may then be disentangled by using frequency-selective radiofrequency pulses. Theoretical results and numerical simulations are compared with experimental data for the C-13 nuclei in [H-2(7), C-13(3),N-15]-L-alanine. (c) 2006 Elsevier B.V. All rights reserved.",
keywords = "ANGLE-SPINNING NMR, DISTANCE MEASUREMENTS, ROTATIONAL-RESONANCE, SYMMETRY PRINCIPLES, SPECTROSCOPY, PEPTIDES, SYSTEMS, SIMULATION, COUPLINGS, SEQUENCES",
author = "Ildefonso Marin-Montesinos and Giulia Mollica and Marina Carravetta and Axel Gansmueller and Giuseppe Pilelo and Matthias Bechmann and Angelika Sebald and Levitt, {Malcolm H.}",
year = "2006",
month = dec,
day = "11",
doi = "10.1016/j.cplett.2006.10.101",
language = "English",
volume = "432",
pages = "572--578",
journal = "Chemical Physics Letters",
issn = "0009-2614",
publisher = "Elsevier",
number = "4-6",

}

RIS (suitable for import to EndNote) - Download

TY - JOUR

T1 - Truncated dipolar recoupling in solid-state nuclear magnetic resonance

AU - Marin-Montesinos, Ildefonso

AU - Mollica, Giulia

AU - Carravetta, Marina

AU - Gansmueller, Axel

AU - Pilelo, Giuseppe

AU - Bechmann, Matthias

AU - Sebald, Angelika

AU - Levitt, Malcolm H.

PY - 2006/12/11

Y1 - 2006/12/11

N2 - We describe a solid-state NMR concept for the estimation of individual spin-spin couplings in strongly-coupled homonuclear spin systems. A radiofrequency pulse sequence, synchronised with the magic-angle sample rotation recouples zero-quantum dipolar interactions as well as a frequency-dispersing interaction such as the chemical shift anisotropy. The combination of these two recoupled interactions causes the spin system to behave in an approximately weakly-coupled fashion. Individual spin-spin couplings may then be disentangled by using frequency-selective radiofrequency pulses. Theoretical results and numerical simulations are compared with experimental data for the C-13 nuclei in [H-2(7), C-13(3),N-15]-L-alanine. (c) 2006 Elsevier B.V. All rights reserved.

AB - We describe a solid-state NMR concept for the estimation of individual spin-spin couplings in strongly-coupled homonuclear spin systems. A radiofrequency pulse sequence, synchronised with the magic-angle sample rotation recouples zero-quantum dipolar interactions as well as a frequency-dispersing interaction such as the chemical shift anisotropy. The combination of these two recoupled interactions causes the spin system to behave in an approximately weakly-coupled fashion. Individual spin-spin couplings may then be disentangled by using frequency-selective radiofrequency pulses. Theoretical results and numerical simulations are compared with experimental data for the C-13 nuclei in [H-2(7), C-13(3),N-15]-L-alanine. (c) 2006 Elsevier B.V. All rights reserved.

KW - ANGLE-SPINNING NMR

KW - DISTANCE MEASUREMENTS

KW - ROTATIONAL-RESONANCE

KW - SYMMETRY PRINCIPLES

KW - SPECTROSCOPY

KW - PEPTIDES

KW - SYSTEMS

KW - SIMULATION

KW - COUPLINGS

KW - SEQUENCES

U2 - 10.1016/j.cplett.2006.10.101

DO - 10.1016/j.cplett.2006.10.101

M3 - Article

VL - 432

SP - 572

EP - 578

JO - Chemical Physics Letters

JF - Chemical Physics Letters

SN - 0009-2614

IS - 4-6

ER -