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X-{H-1, F-19} triple resonance with a X-{H-1} CP MAS probe and characterisation of a Si-29-F-19 spin pair

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X-{H-1, F-19} triple resonance with a X-{H-1} CP MAS probe and characterisation of a Si-29-F-19 spin pair. / Bechmann, M ; Hain, K ; Marichal, C ; Sebald, A .

In: SOLID STATE NUCLEAR MAGNETIC RESONANCE, Vol. 23, No. 1-2, 2003, p. 50-61.

Research output: Contribution to journalArticle

Harvard

Bechmann, M, Hain, K, Marichal, C & Sebald, A 2003, 'X-{H-1, F-19} triple resonance with a X-{H-1} CP MAS probe and characterisation of a Si-29-F-19 spin pair', SOLID STATE NUCLEAR MAGNETIC RESONANCE, vol. 23, no. 1-2, pp. 50-61. https://doi.org/10.1016/S0926-2040(02)00014-0

APA

Bechmann, M., Hain, K., Marichal, C., & Sebald, A. (2003). X-{H-1, F-19} triple resonance with a X-{H-1} CP MAS probe and characterisation of a Si-29-F-19 spin pair. SOLID STATE NUCLEAR MAGNETIC RESONANCE, 23(1-2), 50-61. https://doi.org/10.1016/S0926-2040(02)00014-0

Vancouver

Bechmann M, Hain K, Marichal C, Sebald A. X-{H-1, F-19} triple resonance with a X-{H-1} CP MAS probe and characterisation of a Si-29-F-19 spin pair. SOLID STATE NUCLEAR MAGNETIC RESONANCE. 2003;23(1-2):50-61. https://doi.org/10.1016/S0926-2040(02)00014-0

Author

Bechmann, M ; Hain, K ; Marichal, C ; Sebald, A . / X-{H-1, F-19} triple resonance with a X-{H-1} CP MAS probe and characterisation of a Si-29-F-19 spin pair. In: SOLID STATE NUCLEAR MAGNETIC RESONANCE. 2003 ; Vol. 23, No. 1-2. pp. 50-61.

Bibtex - Download

@article{1d263e45acc84ffaa8b9a87224d05130,
title = "X-{H-1, F-19} triple resonance with a X-{H-1} CP MAS probe and characterisation of a Si-29-F-19 spin pair",
abstract = "An economic approach for implementing X-{H-1, F-19} double-decoupling MAS NMR experiments with a conventional X-{H-1} dual-channel CP MAS probe is demonstrated. The parameters characterising the isolated Si-29-F-19 spin pair in an organosilicon compound R3SiF (R = 9-anthryl) are determined. In addition, we discuss the optimum choice of experimental parameters for determining all Si-29-F-19 spin-pair parameters from straightforward Si-29 MAS NMR spectra with only H-1 decoupling applied during acquisition. (C) 2002 Elsevier Science (USA). All rights reserved.",
keywords = "{H-1,F-19} double-decoupling MAS NMR, Si-29-F-19 spin pair, NUCLEAR-MAGNETIC-RESONANCE, NMR",
author = "M Bechmann and K Hain and C Marichal and A Sebald",
year = "2003",
doi = "10.1016/S0926-2040(02)00014-0",
language = "English",
volume = "23",
pages = "50--61",
journal = "SOLID STATE NUCLEAR MAGNETIC RESONANCE",
issn = "0926-2040",
publisher = "Elsevier",
number = "1-2",

}

RIS (suitable for import to EndNote) - Download

TY - JOUR

T1 - X-{H-1, F-19} triple resonance with a X-{H-1} CP MAS probe and characterisation of a Si-29-F-19 spin pair

AU - Bechmann, M

AU - Hain, K

AU - Marichal, C

AU - Sebald, A

PY - 2003

Y1 - 2003

N2 - An economic approach for implementing X-{H-1, F-19} double-decoupling MAS NMR experiments with a conventional X-{H-1} dual-channel CP MAS probe is demonstrated. The parameters characterising the isolated Si-29-F-19 spin pair in an organosilicon compound R3SiF (R = 9-anthryl) are determined. In addition, we discuss the optimum choice of experimental parameters for determining all Si-29-F-19 spin-pair parameters from straightforward Si-29 MAS NMR spectra with only H-1 decoupling applied during acquisition. (C) 2002 Elsevier Science (USA). All rights reserved.

AB - An economic approach for implementing X-{H-1, F-19} double-decoupling MAS NMR experiments with a conventional X-{H-1} dual-channel CP MAS probe is demonstrated. The parameters characterising the isolated Si-29-F-19 spin pair in an organosilicon compound R3SiF (R = 9-anthryl) are determined. In addition, we discuss the optimum choice of experimental parameters for determining all Si-29-F-19 spin-pair parameters from straightforward Si-29 MAS NMR spectra with only H-1 decoupling applied during acquisition. (C) 2002 Elsevier Science (USA). All rights reserved.

KW - {H-1,F-19} double-decoupling MAS NMR

KW - Si-29-F-19 spin pair

KW - NUCLEAR-MAGNETIC-RESONANCE

KW - NMR

U2 - 10.1016/S0926-2040(02)00014-0

DO - 10.1016/S0926-2040(02)00014-0

M3 - Article

VL - 23

SP - 50

EP - 61

JO - SOLID STATE NUCLEAR MAGNETIC RESONANCE

JF - SOLID STATE NUCLEAR MAGNETIC RESONANCE

SN - 0926-2040

IS - 1-2

ER -